Thermal Post-Processing of 3D Printed Polypropylene Parts for Vacuum Systems

Access to vacuum systems is limited because of economic costs. A rapidly growing approach to reduce the costs of scientific equipment is to combine open-source hardware methods with digital distributed manufacturing with 3D printers. Although high-end 3D printers can manufacture vacuum components, again, the cost of access to tooling is economically prohibitive. Low-cost material extrusion 3D printing with plastic overcomes the cost issue, but two problems arise when attempting to use plastic in or as part of vacuum systems: the outgassing of polymers and their sealing. To overcome these challenges, this study explores the potential of using post-processing heat treatments to seal 3D printed polypropylene for use in vacuum environments. The effect of infill overlap and heat treatment with a readily available heat gun on 3D printed PP parts was investigated in detail on ISO-standardized KF vacuum fitting parts and with the use of computer vision-based monitoring of vacuum pump down velocities. The results showed that infill overlap and heat treatment both had a large impact on the vacuum pressures obtainable with 3D printed parts. Heat treatment combined with 98% infill reliably sealed parts for use in vacuum systems, which makes the use of low-cost desktop 3D printers viable for manufacturing vacuum components for open scientific hardware.